1-甲基-2-硝基-1H-咪唑合成路线 (共 8 条)
反应条件
nitronium tetrafluoroborate in nitromethane T=-20 - 125°C; 3.16667 h; Product distribution / selectivity;
参考文献
US7304164 B1, ;
Page/Page column 7 ;
反应条件
sodium hydrogencarbonate in water T=60 - 65°C;
参考文献
New Journal of Chemistry, , vol. 30, # 3 p. 349 - 358
反应条件
sulfuric acid; sulfur trioxide; nitric acid T=110 - 120°C; 2 h; Product distribution / selectivity;
参考文献
US7304164 B1, ;
Page/Page column 7 ;
反应条件
nitronium tetrafluoroborate in nitromethane T=-20 - 125°C;
参考文献
Synthesis, , # 17 art. no. M43211SS, p. 2859 - 2864
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=20°C; 48 h;
参考文献
Palmer, Brian D.; Denny, William A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 95 - 99
反应条件
bromine in 1,4-dioxane 144 h; Ambient temperature;
参考文献
Farah, Salim F.; McClelland, Robert A.
Canadian Journal of Chemistry, 1993 , vol. 71, # 4 p. 427 - 432
参考文献
Lee; Palmer; Wilson; Denny
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 13 p. 1741 - 1744
反应条件
phosphate buffer in water-d2
electrochemical reduction, chemical reduction (zinc, ammonium chloride),irradiation; Product distribution;
参考文献
Clelland, Robert A. Mc; Panicucci, Rick; Rauth, A. Michael
Journal of the American Chemical Society, 1987 , vol. 109, # 14 p. 4308 - 4314