N-(2-氯乙基)-N-甲基苯胺合成路线 (共 13 条)
反应条件
thionyl chloride in dichloromethane 1 h; Reflux;
参考文献
CINCINNATI CHILDREN'S HOSPITAL MEDICAL CENTER; UNIVERSITY OF CINCINNATI; Merino, Edward J.; Mulloy, James C.; Li, Guorui; Bell-Horwath, Tiffany
Patent: US2013/230542 A1, 2013 ;
Location in patent: Paragraph 0123 ;
反应条件
trimethylamine borane in xylene 7 h; Heating;
参考文献
Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea
Synthesis, 1983 , # 12 p. 1013 - 1014
反应条件
sodium carbonate in butanone 30 h; Heating;
参考文献
Corsano, S; Strappaghetti, G; Codagnone, A; Scapicchi, R; Marucci, G
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 5 p. 545 - 549
反应条件
ethylmagnesium bromide Umsertzung des Reaktionsprodukts mit p-Toluolsulfonsaeure-<β-chlor-aethylester>;
参考文献
CINCINNATI CHILDREN'S HOSPITAL MEDICAL CENTER; UNIVERSITY OF CINCINNATI; Merino, Edward J.; Mulloy, James C.; Li, Guorui; Bell-Horwath, Tiffany
Patent: US2013/230542 A1, 2013 ;
参考文献
v.Braun; Kirschbaum
Chemische Berichte, 1919 , vol. 52, p. 1719
参考文献
Clemo; Perkin
Journal of the Chemical Society, 1922 , vol. 121, p. 664
参考文献
v.Braun; Kirschbaum
Chemische Berichte, 1919 , vol. 52, p. 1719
反应条件
trichlorophosphate; benzene
参考文献
I.G. Farbenind.
Patent: DE711665 , 1935 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Gen. Aniline Works
Patent: US2141090 , 1936 ;
Full Text Show Details
Anker; Cook
Journal of the Chemical Society, 1944 , p. 489,491
反应条件
1: benzene; phosphorus oxychloride 2: aq.-ethanolic sodium carbonate View Scheme
参考文献
I.G. Farbenind.
Patent: DE711665 , 1935 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Gen. Aniline Works
Patent: US2141090 , 1936 ;
参考文献
I.G.Farbenind.
Patent: DE488945 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 2697