3-(4-甲基苯基)-1-苯基-1-丙酮合成路线 (共 23 条)
反应条件
sodium hydride in tetrahydrofuran 3.5 h; Inert atmosphereRefluxSchlenk technique;
参考文献
Yang, Dongmei; Zhou, Yuhan; Xue, Na; Qu, Jingping
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4171 - 4176
反应条件
hydrogen in water
T=25°C; 2 h; chemoselective reaction;
参考文献
Ding, Boqiang; Zhang, Zhenfeng; Liu, Yangang; Sugiya, Masashi; Imamoto, Tsuneo; Zhang, Wanbin
Organic Letters, 2013 , vol. 15, # 14 p. 3690 - 3693
反应条件
triphenyl-arsane; hydrogen; N-ethyl-N,N-diisopropylamine; [RhCl(cycloocta-1,5-diene)2]B(3,5-(CF3)2C6H3)4 in diethylene glycol dimethyl ether
T=65°C; P=760 Torr;
参考文献
Hong, Young-Taek; Barchuk, Andriy; Krische, Michael J.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 41 p. 6885 - 6888
反应条件
tris-(dibenzylideneacetone)dipalladium(0); CsOH; 2,6-bis(N-butyl-N'-methylenebenzimidazolium)-1-bromophenylene dibromide in para-xylene
T=125°C; Inert atmosphere;
参考文献
Kose, Osamu; Saito, Susumu
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 4 p. 896 - 900
反应条件
lithium tert-butylate in toluene
T=110°C; 12 h; Inert atmosphere;
参考文献
Liang, Yu-Feng; Zhou, Xin-Feng; Tang, Shi-Ya; Huang, Yao-Bing; Feng, Yi-Si; Xu, Hua-Jian
RSC Advances, 2013 , vol. 3, # 21 p. 7739 - 7742
反应条件
palladium 10 on activated carbon; sodium carbonate in ethanol; water
T=100°C; Heck Reaction; 6 h;
参考文献
Kim, Hyun-Soo; Lee, Sang-Jin; Yoon, Cheol Min
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 325 - 327
反应条件
C42H36ClIrO2P2; potassium hydroxide in para-xylene
T=130°C; 12 h; Inert atmosphereSchlenk techniqueMolecular sieve; Reagent/catalyst;
参考文献
Musa, Sanaa; Ackermann, Lutz; Gelman, Dmitri
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 3077 - 3080
反应条件
potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Shim, Sang Chul
Journal of Organometallic Chemistry, 2006 , vol. 691, # 20 p. 4329 - 4332
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane
T=60°C; P=750.075 Torr; 20 h; Inert atmosphere;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880
反应条件
ammonium acetate; zinc in ethanol
T=20°C; 1.75 h;
参考文献
Zhou, Yong-Bo; Wang, Yu-Iu; Wang, Jin-Ye
Journal of Chemical Research, 2004 , # 2 p. 118 - 119