(4-甲氧基吡啶-2-基)甲醇合成路线 (共 21 条)
反应条件
1: With trifluoroacetic anhydride in dichloromethane T=0 - 40°C; 6.83 h; 2: With water; sodium hydrogencarbonate in dichloromethane 1 h;
参考文献
WO2009/56886 A1, ;
Page/Page column 54 ;
WO 2009/056886 A1
反应条件
potassium carbonate in hydrogenchloride
反应条件
1: With lithium aluminium tetrahydride in diethyl ether T=20°C; 1 h; 2: With water; Potassium sodium tartrate in diethyl ether
参考文献
US7081461 B1, ;
Page/Page column 45 ;
US 7081461 B1
反应条件
(NH4)2S2O8 in methanol; dichloromethane (CH2 Cl2); water
参考文献
US5972972 A1, ;
US 5972972 A
反应条件
1: H2SO4; HNO3 2: acetic anhydride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 17 p. 5186 - 5192
反应条件
1: acetic anhydride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 17 p. 5186 - 5192
反应条件
in methanol T=80°C; 24 h; Reflux;
参考文献
Inorganic Chemistry, , vol. 52, # 11 p. 6481 - 6501
反应条件
sulfuric acid; water 1 h; Heating;
参考文献
Journal of Chemical Research, Miniprint, , # 6 p. 1341 - 1350
反应条件
1: CH2Cl2 / 1.5 h / Ambient temperature 2: aq. (NH4)2S2O8 / 1 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 19, # 1, 2 p. 317 - 326