二甲基2,2'-二硫烷二基二乙酸酯合成路线 (共 14 条)
反应条件
water Product distribution;
参考文献
Andreeva, I. A.; Mandel'baum, Ya. A.; Soifer, R. S.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 6 p. 1322 - 1325,1072 - 1075
反应条件
magnesium in methanol 2 h; Ambient temperature;
参考文献
Sridhar, Madabhushi; Vadivel, Subramanian K.; Bhalerao, Uday T.
Synthetic Communications, 1997 , vol. 27, # 8 p. 1347 - 1350
反应条件
phosphorous acid trisdiethylamide in benzene Ambient temperature;
参考文献
Harpp; Gleason
The Journal of organic chemistry, 1971 , vol. 36, # 1 p. 73 - 80
参考文献
Hamel, Pierre; Girard, Mario
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1695 - 1701
反应条件
pyridine; sulfuryl dichloride in dichloromethane 1) -70 --> 0 deg C; 2) 0 deg C, 10 min;
参考文献
Bachi, Mario D.; Bar-Ner, Nira; Melman, Artem
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7116 - 7124
反应条件
ammonium cerium(IV) nitrate in acetonitrile
0.333333 h;
参考文献
Salehi, Peyman; Ali Zolfigol, Mohammad Ali; Tolami, Leila Bazaz
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 9 p. 1777 - 1781
反应条件
acetyl chloride
16 h; Heating;
参考文献
Bigham, Eric C.; Mallory, W. Revill; Hodson, Steven J.; Duch, David S.; Ferone, Robert; Smith, Gary K.
Heterocycles, 1993 , vol. 35, # 2 p. 1289 - 1307
反应条件
2,2'-azo-bisisobutyronitrile in toluene
T=80°C; Inert atmosphere; optical yield given as percent de;
参考文献
Minozzi, Matteo; Monesi, Alessandro; Nanni, Daniele; Spagnolo, Piero; Marchetti, Nicola; Massi, Alessandro
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 450 - 459
反应条件
in benzene
T=20°C; 6 h;
参考文献
Andreeva, I. A.; Soifer, R. S.; Mandel'baum, Ya. A.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 6 p. 1325 - 1329,1075 - 1078
反应条件
1,2-diphenyl-1-keto-2,2-dimethoxyethane in dimethyl sulfoxide
T=20 - 40°C; UV-irradiation; optical yield given as percent de;
参考文献
Minozzi, Matteo; Monesi, Alessandro; Nanni, Daniele; Spagnolo, Piero; Marchetti, Nicola; Massi, Alessandro
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 450 - 459