(2-氨基乙基)甲基(苯)胺 1HCL合成路线 （共 21 条）
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 1 h;
参考文献
Murahashi, Shun-Ichi; Komiya, Naruyoshi; Terai, Hiroyuki; Nakae, Takahiro
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15312 - 15313
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 1 h;
参考文献
Murahashi, Shun-Ichi; Nakae, Takahiro; Terai, Hiroyuki; Komiya, Naruyoshi
Journal of the American Chemical Society, 2008 , vol. 130, # 33 p. 11005 - 11012
反应条件
ammonia in methanol 1.) 0 deg C, 2 h 2.) rt, 2 h;
参考文献
Wimalasena, Kandatege; May, Sheldon W.
Journal of the American Chemical Society, 1987 , vol. 109, # 13 p. 4036 - 4046
反应条件
in neat (no solvent) T=150 - 165°C;
参考文献
Poindexter, Graham S.; Owens, Donald A.; Dolan, Peter L.; Woo, Edmund
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6257 - 6265
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 48 h; Heating;
参考文献
Lewis, Frederick D.; Burch, Erick L.
Journal of Physical Chemistry, 1996 , vol. 100, # 10 p. 4055 - 4063
反应条件
1: 86 percent / Et3N / 2 h / Ambient temperature 2: 75 percent / NH3(g) / methanol / 1.) 0 deg C, 2 h 2.) rt, 2 h View Scheme
参考文献
Wimalasena, Kandatege; May, Sheldon W.
Journal of the American Chemical Society, 1987 , vol. 109, # 13 p. 4036 - 4046
反应条件
aluminium trichloride; benzene T=90°C;
参考文献
Coleman; Callen
Journal of the American Chemical Society, 1946 , vol. 68, p. 2006
反应条件
xylene beim Erhitzen des Reaktionsprodukts mit wss.HCl;
参考文献
Archer et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5783
反应条件
kieselguhr; ethanol; nickel T=75°C; P=36775.4 Torr; Hydrogenation;
参考文献
I.G.Farbenind.
Patent: DE561156 , 1930 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2998
参考文献
Yamanouchi Pharmaceutical Co., Ltd.
Patent: US4041032 A1, 1977 ;
