2-乙酰基-2'-羟基苯乙酮合成路线 (共 27 条)
反应条件
sodium
4 h; Heating;
参考文献
Sequin, Urs
Helvetica Chimica Acta, 1981 , vol. 64, # 8 p. 2654 - 2664
参考文献
Wittig
Justus Liebigs Annalen der Chemie, 1926 , vol. 446, p. 179
参考文献
Harries
Chemische Berichte, 1891 , vol. 24, p. 3180
参考文献
Dunne et al.
Journal of the Chemical Society, 1950 , p. 1252,1257
反应条件
sodium formate in tetrahydrofuran
T=20°C; Kostanecki-Robinson reaction; 24 h; Inert atmosphere;
参考文献
Stubbing, Louise A.; Li, Freda F.; Furkert, Daniel P.; Caprio, Vittorio E.; Brimble, Margaret A.
Tetrahedron, 2012 , vol. 68, # 34 p. 6948 - 6956
参考文献
Ghosh, Chandra Kanta; Sahana, Sirin; Patra, Amarendra
Tetrahedron, 1993 , vol. 49, # 19 p. 4127 - 4134
反应条件
1: With bromine in ethanol
T=20°C; 2 h;
2: With hydrogenchloride in ethanol
2 h; Heating;
参考文献
Santos, Clementina M. M.; Silva, Artur M. S.; Cavaleiro, Jose A. S.
Synlett, 2005 , # 20 art. no. D29105ST, p. 3095 - 3098
反应条件
bromine in chloroform
2.5 h; Irradiation;
参考文献
Garg, S.; Ishar, M. P. S.; Sarin, R.; Gandhi, R. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 12 p. 1123 - 1128
反应条件
in chloroform
18 h; Yield given;
参考文献
Costes, Jean-Pierre; Fenton, David E.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 2235 - 2240
反应条件
in benzene
6 h; Heatingalso in methanol; Product distributionMechanism;
参考文献
Ghosh, Chandra Kanta; Bhattacharya, Atanu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 7 p. 668 - 670