双(2-二苯基磷苯基)醚合成路线 （共 10 条）
反应条件
1: diphenylether With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; hexane T=20°C; 16 h; 2: chloro-diphenylphosphine in tetrahydrofuran; hexane; Petroleum ether T=20°C; 24 h;
参考文献
Veits; Mutsenek; Neganova; Beletskaya
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 11 p. 1583 - 1586
反应条件
1: diphenylether With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; hexane T=20°C; 16 h; Inert atmosphere; 2: chloro-diphenylphosphine in tetrahydrofuran; hexane T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 1 p. 141 - 154
反应条件
in dichloromethane T=20°C; 3.5 h;
参考文献
Zhang, Peng; Wolf, Christian
Chemical Communications, 2013 , vol. 49, # 62 p. 7010 - 7012
反应条件
in tetrahydrofuran N2 atmosphere, stirring (room temp., overnight); removement of solvent (vacuum), washing (Et2O), drying (vacuum);
参考文献
Kranenburg, Mirko; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
European Journal of Inorganic Chemistry, 1998 , # 2 p. 155 - 157
反应条件
in hydrogenchloride; ethanol (Ar); placing of (C6H4PPh2)2O and abs. EtOH in flask; slow addn. of soln. of PdCl2 in dilute HCl with stirring; stirring for 3 h at 60°C; crystn. overnight, filtration, washing with water, EtOH and ether, drying in vac.;
参考文献
Veits; Mutsenek
Russian Journal of General Chemistry, 2005 , vol. 75, # 2 p. 207 - 211
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate in toluene
参考文献
University of Tennessee Research Foundation
Patent: US2005/124596 A1, 2005 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate in toluene
参考文献
University of Tennessee Research Foundation
Patent: US2005/124596 A1, 2005 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate in toluene
参考文献
University of Tennessee Research Foundation
Patent: US2005/124596 A1, 2005 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate in toluene
参考文献
University of Tennessee Research Foundation
Patent: US2005/124596 A1, 2005 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate in toluene
参考文献
University of Tennessee Research Foundation
Patent: US2005/124596 A1, 2005 ;
