1: 3,6,9,12-tetraoxatetradecane-1,14-diol With sodium in tetrahydrofuran
1.5 h;
2: 2-Propenoic acid tert-butyl ester in tetrahydrofuran
Michael addition;
参考文献
Wosnick, Jordan H.; Mello, Charlene M.; Swager, Timothy M.
Journal of the American Chemical Society, 2005 , vol. 127, # 10 p. 3400 - 3405