2,3-二氢-2-苯基-4(1H)-喹啉合成路线 （共 28 条）
反应条件
antimony trichloride in acetonitrile T=55°C; intramolecular aza-Michael reaction; 3 h;
参考文献
Zheng, Xuxu; Jiang, Heyan; Xie, Jingjing; Yin, Zhongyi; Zhang, Haidong
Synthetic Communications, 2013 , vol. 43, # 7 p. 1023 - 1029
反应条件
phosphoric acid; acetic acid 0.25 h; Heating;
参考文献
Donnelly, John A.; Farrell, David F.
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1757 - 1761
反应条件
silica chloride 0.416667 h; Microwave irradiationNeat (no solvent);
参考文献
Muthukrishnan; Mujahid; Punitharasu; Dnyaneshwar
Synthetic Communications, 2010 , vol. 40, # 9 p. 1391 - 1398
反应条件
hydrogen; palladium on activated charcoal in methanol Ambient temperature;
参考文献
Beifuss, Uwe; Ledderhose, Sabine
Synlett, 1997 , vol. 1997, # 3 p. 313 - 315
反应条件
hydrogen; palladium on activated charcoal in methanol Ambient temperature;
参考文献
Beifuss, Uwe; Ledderhose, Sabine
Synlett, 1997 , vol. 1997, # 3 p. 313 - 315
反应条件
4 A molecular sieve; NAP-MgO in toluene Claisen-Schmidt condensation; 15 h; Heating;
参考文献
Choudary, Boyapati M.; Kantam, Mannepalli L.; Ranganath, Kalluri V. S.; Mahendar, Koosam; Sreedhar, Bojja
Journal of the American Chemical Society, 2004 , vol. 126, # 11 p. 3396 - 3397
反应条件
1: 86 percent / aq. NaOH / ethanol / 3 h / 20 °C 2: 68 percent / H3PO4; AcOH / 1 h / 90 °C View Scheme
参考文献
Synlett, , # 17 p. 2791 - 2794
反应条件
1: With hydrogenchloride T=80 - 85°C; Inert atmosphere; 2: With iron T=100°C; 0.5 h; Inert atmosphere;
参考文献
Bunce, Richard A.; Nammalwar, Baskar
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 3 p. 613 - 619
反应条件
tri-ruthenium(0)dodecacarbonyl; carbon monoxide; DIAN-Me in ethanol; water T=170°C; P=22800 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 15 p. 1741 - 1742
反应条件
1: 68 percent / Et3N / (Ph3P)2PdCl2 / 24 h / 20 °C 2: 89 percent / p-toluenesulfonic acid / benzene / 48 h / 20 °C 3: aq. sodium hydroxide / ethanol / 40 h / 20 °C 4: phosphoric acid / acetic acid / 0.42 h / 90 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 39 p. 13397 - 13418
