1,1,3-三氯五氟丙烷合成路线 (共 11 条)
反应条件
aluminium trichloride T=80°C;
参考文献
Coffman; Cramer; Rigby
Journal of the American Chemical Society, 1949 , vol. 71, p. 979,980
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2462402 , 1945 ;
反应条件
antimony dichloride trifluoride T=250°C;
参考文献
Baker; Whaley
Journal of the American Chemical Society, 1951 , vol. 73, p. 4010
反应条件
hydrogen fluoride; mercury(II) oxide T=190°C; 26 h; Further byproducts given;
参考文献
Fainberg,A.H.; Miller,W.T.
Journal of Organic Chemistry, 1965 , vol. 30, p. 864 - 876
反应条件
d-limonene; aluminum chlorofluoride T=15.4 - 40.2°C; P=1085.86 Torr; 0.72 h; Product distribution / selectivity;
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/54780 A2, 2008 ;
Location in patent: Page/Page column 17 ;
反应条件
hydrogen fluoride; chlorine; CrO3/C T=235 - 435°C;
参考文献
Belter, Randolph K.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 5 p. 552 - 556
反应条件
aluminum chlorofluoride T=37 - 41°C; P=3759.59 Torr; 4 h; Product distribution / selectivity;
参考文献
E.I.DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/54780 A2, 2008 ;
Location in patent: Page/Page column 16-17 ;
反应条件
AlClxF3-x T=60 - 80°C; P=4897.34 - 6759.13 Torr; 2.55 h; Sealed tube; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/79525 A2, 2009 ;
Location in patent: Page/Page column 14 ;
反应条件
SbF3; chlorine T=185°C;
参考文献
Minnesota Mining and Mfg.Co.
Patent: US2880247 , 1955 ;
反应条件
SbF3; chlorine T=185°C;
参考文献
Minnesota Mining and Mfg.Co.
Patent: US2880247 , 1955 ;
反应条件
T=80°C; unter Druck;
参考文献
Coffman; Cramer; Rigby
Journal of the American Chemical Society, 1949 , vol. 71, p. 979,980
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2462402 , 1945 ;