in neat (no solvent) to silyl-substituted ethylene was slowly added dropwise with stirring HGeCl3*2Et2O; ppt. was formed; mixt. heated at 50°C for 5 h; isolated by vac. distn.;
参考文献
Lakhtin; Knyazev; Pavlov; Gusel'nikov; Buravtseva; Kuyantseva; Parshkova; Mid'ko; Bykovchenko; Kisin; Chernyshev
Russian Journal of General Chemistry, 2008 , vol. 78, # 5 p. 898 - 902