2-溴甲基-4-氰基苯甲酸甲酯合成路线 (共 3 条)
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
US5591752 A1, ;
US 5591752 A
反应条件
1: 5 h / 180 °C / |Inert atmosphere 2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 3 h / |Inert atmosphere; |Reflux View Scheme
反应条件
1: thionyl chloride / 2 h / 70 °C / |Inert atmosphere 2: 5 h / 180 °C / |Inert atmosphere 3: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 3 h / |Inert atmosphere; |Reflux View Scheme