1,2,3-三苯基环丙烯合成路线 (共 17 条)
反应条件
1: LiNH2, liq. NH3 2: 280 °C View Scheme
参考文献
Breslow,R.; Dowd,P.
Journal of the American Chemical Society, 1963 , vol. 85, p. 2729 - 2735
反应条件
in benzene 72 h; Heating;
参考文献
Jens, Klaus-Joachim; Weiss, Erwin
Chemische Berichte, 1984 , vol. 117, # 7 p. 2469 - 2478
反应条件
bis(acetylacetonate)nickel(II); ethyl magnesium chloride in tetrahydrofuran; diethyl ether 1.) 25 deg C, 3 h; 2.) reflux, 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 512, # 1-2 p. 207 - 217
反应条件
bis(acetylacetonate)nickel(II); ethyl magnesium chloride in tetrahydrofuran; diethyl ether 1.) 25 deg C, 3 h; 2.) reflux, 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 512, # 1-2 p. 207 - 217
反应条件
aluminium trichloride in dichloromethane
T=-78 - 20°C;
参考文献
Bartmann, Ekkehard; Gompper, Rudolf
Synthetic Communications, 1987 , vol. 17, # 3 p. 263 - 270
反应条件
hexacarbonyl molybdenum; carbon monoxide in 1,4-dioxane
P=836 Torr; 22 h; Heating;
参考文献
Semmelhack; Ho, Suzzy; Cohen; Steigerwald; Lee; Gilbert, Adam M.; Wutff, William D.; Ball, Richard G.
Journal of the American Chemical Society, 1994 , vol. 116, # 16 p. 7108 - 7122
反应条件
PPh3 gold(I) chloro complex; silver trifluoromethanesulfonate in dichloromethane
T=20°C; 0.5 h;
参考文献
Li, Changkun; Zeng, Yi; Wang, Jianbo
Tetrahedron Letters, 2009 , vol. 50, # 24 p. 2956 - 2959
反应条件
in 1,4-dioxane
1 h; Heating;
参考文献
Semmelhack; Ho, Suzzy; Cohen; Steigerwald; Lee; Gilbert, Adam M.; Wutff, William D.; Ball, Richard G.
Journal of the American Chemical Society, 1994 , vol. 116, # 16 p. 7108 - 7122
反应条件
in pentane
T=-10°C; 9 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Klett,M.W.; Johnson,R.P.
Journal of the American Chemical Society, 1985 , vol. 107, p. 3963
反应条件
aluminium trichloride in dichloromethane
T=-78 - 20°C;
参考文献
Bartmann, Ekkehard; Gompper, Rudolf
Synthetic Communications, 1987 , vol. 17, # 3 p. 263 - 270