3-丁氧基-2-环己烯-1-酮合成路线 (共 6 条)
反应条件
iodine T=20°C; 0.0666667 h;
参考文献
Bhosale, Rajesh S.; Bhosale, Sidhanath V.; Bhosale, Sheshanath V.; Wang, Tianyu; Zubaidha
Tetrahedron Letters, 2004 , vol. 45, # 39 p. 7187 - 7188
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1.5 h; Heating;
参考文献
Middleton, Donald S.; Simpkins, Nigel S.; Begley, Michael J.; Terrett, Nicholas K.
Tetrahedron, 1990 , vol. 46, # 2 p. 545 - 564
反应条件
1: hex-5-ynoic acid With oxalyl dichloride in dichloromethane 2.5 h; Inert atmosphere; 2: With indium(III) chloride in dichloromethane 3 h; Inert atmosphere; 3: butan-1-ol in dichloromethane Inert atmosphere;
参考文献
Hylden, Anne T.; Uzelac, Eric J.; Ostojic, Zeljko; Wu, Ting-Ting; Sacry, Keely L.; Sacry, Krista L.; Xi, Lin; Jones, T. Nicholas
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1323 - 1326
反应条件
potassium ethanolate
参考文献
Stetter; Dierichs
Chemische Berichte, 1952 , vol. 85, p. 61,71
反应条件
dichloro bis(acetonitrile) palladium(II) T=20°C; P=15 Torr; 6 h; Product distribution / selectivity;
参考文献
Mitsubishi Chemical Corporation
Patent: JP2005/170912 A, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile 0.75 h; Heating;
参考文献
Banerjee, Biplab; Mandal, Samir Kumar; Roy, Subhas Chandra
Chemistry Letters, 2006 , vol. 35, # 1 p. 16 - 17