1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 合成路线 （共 53 条）
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
反应条件
ytterbium trichloride; zinc in tetrahydrofuran T=50 - 67°C; 0.416667 h;
参考文献
Huang, Wei-Yuan; Zhao, Gang; Ding, Yu
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
lead(II) bromide; aluminium 1 h; Ambient temperature;
参考文献
Hu, Chang-Ming; Tang, Xiao-Qing
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
反应条件
in N,N-dimethyl-formamide T=60°C; 10 h;
参考文献
Chen, Qing-Yun; Qiu, Zai-Ming
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
in N,N-dimethyl-formamide T=60°C; 10 h;
参考文献
Chen, Qing-Yun; Qiu, Zai-Ming
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
反应条件
lithium aluminium tetrahydride in diethyl ether 20 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Chen, Quing-Yun; Chen, Ming-Fang
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h; other catalysts, other tertiary amines, other polyfluoroalkyl iodides, var. times and temp.; Product distributionMechanism;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
potassium carbonate in N,N-dimethyl-formamide 16 h; Irradiation;
参考文献
Zhou, Qi-Lin; Huang, Yao-Zeng
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
di-tert-butylnitroxide radical; sodium hydride 1.) DMF, 2.) DMF, 70 deg C, 10h, irradiation; Yield given. Multistep reaction;
参考文献
Chen, Qing-Yun; Chen, Mei-Jin
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
di-tert-butylnitroxide radical; sodium hydride 1.) DMF, 2.) DMF, 70 deg C, 10h, irradiation; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chen, Qing-Yun; Chen, Mei-Jin
16486-97-8 1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷 +
→
反应条件
反应条件
sodium hydride 1.) DMF, 2.) DMF, 70 deg C, 10h, irradiation; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chen, Qing-Yun; Chen, Mei-Jin
