1-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷合成路线 （共 53 条）
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷+
→
反应条件
[Co(HDm)2Py]Br; zinc in ethanol T=30°C; 5 h;
参考文献
Hu, Chan-Ming; Qiu, Yao-Ling
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3339 - 3342
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
sodium; ethyl acetoacetate in ethanol; N,N-dimethyl-formamide T=75°C; 10 h;
参考文献
CHEN,Q.Y.; QUI,Z.M.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 343
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
magnesium in tetrahydrofuran 5 h; Heating;
参考文献
Chen, Quing-Yun; Qiu, Zai-Ming; Yang, Zhen-Yu
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 149 - 162
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
tetrakis(triphenylphosphine) palladium(0) in hexane T=60°C; 0.5 h;
参考文献
Huang, Yao-Zeng; Shou, Qi-Lin
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3552 - 3558
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
lithium aluminium tetrahydride in diethyl ether T=10°C; 13 h;
参考文献
Chen, Quing-Yun; Chen, Ming-Fang
Journal of Fluorine Chemistry, 1990 , vol. 49, # 1 p. 107 - 114
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
→
反应条件
lithium aluminium tetrahydride in diethyl ether T=10°C; 13 h;
参考文献
Chen, Quing-Yun; Chen, Ming-Fang
Journal of Fluorine Chemistry, 1990 , vol. 49, # 1 p. 107 - 114
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷+
→
反应条件
potassium carbonate in N,N-dimethyl-formamide 14 h; Irradiation;
参考文献
Zhou, Qi-Lin; Huang, Yao-Zeng
Journal of Fluorine Chemistry, 1988 , vol. 39, p. 87 - 98
