2,2,2-三氟乙烷磺酰氯合成路线 （共 9 条）
反应条件
chlorine in water T=-5 - 0°C; oxidative chlorination; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 46, # 16 p. 3335 - 3336
反应条件
chlorine in hydrogenchloride T=-30 - -25°C; 0.5 h;
参考文献
Chemische Berichte, , vol. 121, p. 1435 - 1440
反应条件
chlorine in water T=-5 - 0°C; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 46, # 16 p. 3335 - 3336
反应条件
hydrogenchloride; chlorine T=0 - 5°C; 0.133333 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 3 p. 808 - 811
反应条件
hydrogenchloride; chlorine 4 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 50, # 8 p. 1239 - 1246
反应条件
aluminium trichloride
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 27, p. 1837 - 1842
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 27, p. 2084 - 2090
反应条件
H2O in water 10 h; Heating;
参考文献
Bunyagidj; Piotrowska; Aldridge
Journal of Chemical and Engineering Data, 1981 , vol. 26, # 3 p. 344 - 346
反应条件
potassium carbonate in dichloromethane; anhydrous amyl acetate; acetone
参考文献
ELI LILLY AND COMPANY
Patent: EP875507 A1, 1998 ;
参考文献
PFIZER LIMITED; BELL, Andrew Simon; DE GROOT, Marcel John; LEWTHWAITE, Russell Andrew; MARSH, Ian Roger; SCIAMMETTA, Nunzio; STORER, Robert Ian; SWAIN, Nigel Alan
Patent: WO2012/95781 A1, 2012 ;
Location in patent: Page/Page column 109 ;
WO 2012/095781 A1
