1,1'-(4-羟基-6-甲基-1,3-亚苯基)二乙酮合成路线 (共 19 条)
参考文献
Knoevenagel
Chemische Berichte, 1903 , vol. 36, p. 2186
反应条件
oxygen; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide
T=100°C; 4.8 h; Green chemistry;
参考文献
Gao, Qi; Tan, Xian-Chun; Pan, Ying-Ming; Wang, Heng-Shan; Liang, Ying
Chemical Communications, 2012 , vol. 48, # 99 p. 12080 - 12081
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Doerner, Thomas; Gleiter, Rolf; Robbins, Timothy A.; Chayangkoon, Paochai; Lightner, David A.
Journal of the American Chemical Society, 1992 , vol. 114, # 9 p. 3235 - 3241
反应条件
ytterbium(III) triflate in carbon disulfide
Friedel-Crafts reaction; 10 h; Heating;
参考文献
Su, Weike; Jin, Can
Synthetic Communications, 2004 , vol. 34, # 22 p. 4199 - 4205
反应条件
potassium hydroxide in methanol
3 h; Heating;
参考文献
Remennikov, G. Ya.; Kurilenko, L. K.; Boldyrev, I. V.; Cherkasov, V. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 4 p. 422 - 425
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 4 p. 508 - 512
反应条件
potassium hydroxide in methanol
5 h; Heating;
参考文献
Remennikov, G. Ya.; Kurilenko, L. K.; Boldyrev, I. V.; Cherkasov, V. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 4 p. 422 - 425
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 4 p. 508 - 512
反应条件
aluminium trichloride
T=165°C; 2.5 h;
参考文献
Khan; Venkatachalam; Hasnain Khan; Javed; Drabu
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 11 p. 1067 - 1069
反应条件
hydrogenchloride; air; chloroform
参考文献
Knoevenagel
Chemische Berichte, 1903 , vol. 36, p. 2186
反应条件
triethylamine
5 h; Heating;
参考文献
Remennikov, G. Ya.; Kurilenko, L. K.; Boldyrev, I. V.; Cherkasov, V. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 4 p. 422 - 425
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 4 p. 508 - 512
反应条件
triethylamine
4 h; Heating;
参考文献
Remennikov, G. Ya.; Kurilenko, L. K.; Boldyrev, I. V.; Cherkasov, V. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 4 p. 422 - 425
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 4 p. 508 - 512