sodium tetrahydroborate 1) 20 deg C, 2) reflux 2 h; Yield given. Title compound not separated from byproducts;
参考文献
Kadzyauskas, P. P.; Malinauskene, Yu. A.; Butkus, E. P.; Zefirov, N. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 727 - 729
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 940 - 942
sodium tetrahydroborate 1) ethanol, reflux, 2 h 2) 20 deg C, 3 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Kadzyauskas, P. P.; Malinauskene, Yu. A.; Butkus, E. P.; Zefirov, N. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 727 - 729
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 940 - 942
1: pyridine / 48 h / 0 °C 2: 1,5-diazabicyclo<5.4.0>undec-5-ene / 100 - 200 °C View Scheme
参考文献
Bishop, Roger; Choudhury, Shamima; Dance, Ian
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1159 - 1168