4,4-二甲基-1-己烯合成路线 （共 15 条）
反应条件
lithium tetrachloroaluminate in diethyl ether T=5°C; 20 h;
参考文献
Beckwith, Athelstan L. J.; Easton, Christopher J.; Lawrence, Tony; Serelis, Algirdas K.
Australian Journal of Chemistry, 1983 , vol. 36, # 3 p. 545 - 556
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1653
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1653
反应条件
1: AlCl3 / -8 - 7 °C 2: zinc; propyl alcohol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1653
反应条件
1: AlCl3 / -30 °C 2: zinc; propyl alcohol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1653
反应条件
1: 1.) cuprous chloride / 1.) ether, -45 deg C, 10 min, 2.) ether, from -35 deg C to RT, 2 h 2: 86 percent / lithium chloride, water / dimethylsulfoxide / 14 h / Heating 3: 88 percent / lithium aluminium hydride 4: 5.5 g / pyridine 5: 54 percent / lithium aluminium chloride / diethyl ether / 20 h / 5 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 36, # 3 p. 545 - 556
反应条件
1: 5.5 g / pyridine 2: 54 percent / lithium aluminium chloride / diethyl ether / 20 h / 5 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 36, # 3 p. 545 - 556
反应条件
1: 86 percent / lithium chloride, water / dimethylsulfoxide / 14 h / Heating 2: 88 percent / lithium aluminium hydride 3: 5.5 g / pyridine 4: 54 percent / lithium aluminium chloride / diethyl ether / 20 h / 5 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 36, # 3 p. 545 - 556
反应条件
1: 88 percent / lithium aluminium hydride 2: 5.5 g / pyridine 3: 54 percent / lithium aluminium chloride / diethyl ether / 20 h / 5 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 36, # 3 p. 545 - 556
反应条件
diethyl ether T=0°C;
