1: salicylaldehyde With potassium hydroxide in ethanol 0.0833333 h; Cooling with ice; 2: chloroacetone in ethanol 0.166667 h; Cooling with ice; 3: With potassium iodide in ethanol T=20°C; 0.333333 h;
参考文献
Goudarshivannanavar; Jayadevappa; Mahadevan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 10 p. 1419 - 1423
1: salicylaldehyde With potassium hydroxide in ethanol Aldol Condensation; 0.25 h; Cooling with ice; 2: 1-bromo-2-propanone With potassium iodide in ethanol Aldol Condensation; Cooling;
参考文献
Aruna Kumar; Desai, Nivedita R.; Krishnaswamy; Sreenivasa; Mahadevan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 426 - 430
1: With N-[(1R,2R)-2-amino-1,2-diphenylethyl]-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-thiourea; 4-nitro-benzoic acid in tetrahydrofuran Michael Addition; 8 h; Reflux; 2: With sodium hydroxide in tetrahydrofuran T=20°C; Michael Addition; 1 h; optical yield given as percent deenantioselective reaction;
