4-(叔丁氧基羰基氨基)苯甲酸甲酯合成路线 （共 10 条）
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in acetonitrile T=20°C;
参考文献
ELI LILLY AND COMPANY
Patent: WO2004/14900 A1, 2004 ;
Location in patent: Page 49 ;
WO 2004/014900 A1
反应条件
triethylsilane; palladium hydroxide - carbon in ethanol T=50°C; 36 h;
参考文献
Kotsuki, Hiyoshizo; Ohishi, Takeshi; Araki, Tomohiro
Tetrahedron Letters, 1997 , vol. 38, # 12 p. 2129 - 2132
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol T=20°C; 3 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol T=20°C; 5 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=100°C; 2 h;
参考文献
Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; Zhu, Zhiwu; Wu, Yusheng
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4445 - 4448
反应条件
silver carbonate in ethylene glycol dimethyl ether T=80°C; 72 h;
参考文献
Lee, Kang-Sang; Lim, Young-Kwan; Cho, Cheon-Gyu
Tetrahedron Letters, 2002 , vol. 43, # 42 p. 7463 - 7464
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
参考文献
The DuPont Merck Pharmaceutical Company
Patent: US5668159 A1, 1997 ;
US 5668159 A
反应条件
1: DMAP / tetrahydrofuran / Heating 2: K2CO3 / methanol / Heating View Scheme
参考文献
Darnbrough; Mervic; Condon; Burns
Synthetic Communications, 2001 , vol. 31, # 21 p. 3273 - 3280
参考文献
The DuPont Merck Pharmaceutical Company
Patent: US5668159 A1, 1997 ;
US 5668159 A
反应条件
HY-Zeolite in dichloromethane 2 h; Heating;
参考文献
Ravindranath; Ramesh; Reddy, M. Ravinder; Das, Biswanath
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 11 p. 1207 - 1208
