4-(三氟甲基)异硫氰酸苯酯合成路线 （共 15 条）
反应条件
triethylamine in tetrahydrofuran T=25°C; 12 h;
参考文献
Wilcox, Craig S.; Kim, Eun-il; Romano, David; Kuo, Lung Huang; Burt, Arthur L.; Curran, Dennis P.
Tetrahedron, 1995 , vol. 51, # 2 p. 621 - 634
反应条件
bis(trichloromethyl) carbonate in chloroform T=0 - 20°C; 4.5 h;
参考文献
Synthetic Communications, , vol. 43, # 24 p. 3342 - 3351
反应条件
acrylic acid methyl ester in water T=20°C; 1.5 h;
参考文献
Jamir, Latonglila; Ali, Abdur Rezzak; Ghosh, Harisadhan; Chipem, Francis A. S.; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 7 p. 1674 - 1678
反应条件
1: With potassium carbonate in water T=40°C; 7 h; Inert atmosphere; 2: With 2,4,6-trichloro-1,3,5-triazine in dichloromethane; water; N,N-dimethyl-formamide T=0°C; Inert atmosphere; 3: With sodium hydroxide in dichloromethane; water pH=11; Inert atmosphere;
参考文献
Sun, Nan; Li, Bin; Shao, Jianping; Mo, Weimin; Hu, Baoxiang; Shen, Zhenlu; Hu, Xinquan
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 61 - 70
反应条件
triethylamine; thiourea in tetrahydrofuran Ambient temperature;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Tetrahedron Letters, 1993 , vol. 34, # 51 p. 8283 - 8284
反应条件
1: sodium hydride / tetrahydrofuran; various solvent(s) / 20 h / 75 °C 2: 63 percent / tosyl chloride; triethylamine / tetrahydrofuran / 0.5 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 10 p. 3969 - 3971
反应条件
1: N-chlorosuccinimide / dimethylformamide; H2O / 0.5 h / Ambient temperature 2: triethylamine / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 9 p. 1597 - 1598
反应条件
triethylamine in tetrahydrofuran Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 9 p. 1597 - 1598
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 12 p. 3916 - 3920
反应条件
in chlorobenzene Heating;
参考文献
Tetrahedron, , vol. 19, p. 1603 - 1610
