2-[(三氟甲基)硫代]溴苯合成路线 （共 4 条）
反应条件
1: 2-bromo-benzenethiol With sodium hydride in N,N-dimethyl-formamide T=20°C; Inert atmosphere; 2: perfluoromethyl iodide in N,N-dimethyl-formamide T=20°C; 14 h;
参考文献
Harsanyi, Antal; Dorko, Eva; Csapo, Agnes; Bako, Tibor; Peltz, Csaba; Rabai, Jozsef
Journal of Fluorine Chemistry, 2011 , vol. 132, # 12 p. 1241 - 1246
反应条件
[2,2']bipyridinyl; potassium carbonate; copper(l) chloride in ethylene glycol dimethyl ether T=45°C; 18 h; Schlenk techniqueInert atmosphereSealed tube;
参考文献
Pluta, Roman; Nikolaienko, Pavlo; Rueping, Magnus
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1650 - 1653
Angew. Chem., 2014 , vol. 126, # 6 p. 1676 - 1679,4
反应条件
in sulfolane T=230°C; 0.166667 h;
参考文献
Quiclet-Sire, Beatrice; Saicic, Radomir N.; Zard, Samir Z.
Tetrahedron Letters, 1996 , vol. 37, # 50 p. 9057 - 9058
反应条件
hydrogen fluoride 200°C; hours;
参考文献
Journal of Organic Chemistry, , vol. 29, p. 898 - 900
