1,2-二氢-4(3H)-苯基-1,5-苯并二氮杂革-2-酮合成路线 （共 22 条）
反应条件
1: 61 percent / toluene / 8 h / Heating 2: 0.3 g / 5 N H2SO4 / methanol / 2 h / Heating View Scheme
参考文献
Puodzhyunaite, B. A.; Yanchene, R. A.; Terent'ev, P. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , p. 311 - 317
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , vol. 24, # 3 p. 380 - 385
反应条件
nickel; ethyl acetate Hydrogenation;
参考文献
Chen, Xing; Zheng, Yongsheng; Shu, Chang; Yuan, Weicheng; Liu, Bo; Zhang, Xiaomei
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9109 - 9115
反应条件
in xylene
T=139°C; 0.166667 h; Irradiation;
参考文献
Bougrin, Khalid; Bennani, A. Kella; Tetouani, Souad Fkih; Soufiaoui, Mohamed
Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8373 - 8376
参考文献
COMMISSAR. A L'ENERG. ATOM. ET AUX ENERG. ALTERN.; INSTITUT CURIE; CENTRE NAT DE LA RECHERCHE SCIENTIFIQUE
Patent: US2011/201601 A1, 2011 ;
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Essassi, El Mokhtar; Salem, Moussa; Viallefont, Philippe
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 890 - 892
反应条件
in acetic acid
T=90°C;
参考文献
Rao; Reddy; Veeranagaiah
Synthesis, 1992 , # 5 p. 446 - 448
反应条件
acetic acid in ethanol
9 h;
参考文献
Solomko, Z. F.; Proshkina, V. N.; Bozhanova, N. Ya.; Loban, S. V.; Babichenko, L. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 2 p. 183 - 185
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 2 p. 223 - 225
反应条件
hydrogenchloride
T=20 - 25°C; 24 h;
参考文献
Tajana; Pennini; Nardi
Farmaco, Edizione Scientifica, 1980 , vol. 35, # 3 p. 181 - 190
反应条件
1: 80 percent / NH2OH*HCl, NaOAc / aq. ethanol / 2 h / Ambient temperature
2: 56 percent / H2 / 10percent Pd/C / ethanol
View Scheme
参考文献
Essassi, El Mokhtar; Salem, Moussa; Viallefont, Philippe
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 890 - 892
反应条件
1: 70 percent / NH2OH*HCl, NaOAc / ethanol; H2O / 0.5 h / Ambient temperature
2: 80 percent / NH2OH*HCl, NaOAc / aq. ethanol / 2 h / Ambient temperature
3: 56 percent / H2 / 10percent Pd/C / ethanol
View Scheme
参考文献
Essassi, El Mokhtar; Salem, Moussa; Viallefont, Philippe
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 890 - 892
