1: N-decylacetamide With triphenyl phosphite; chlorine; triethylamine in dichloromethane T=-30°C; 2: methanol in dichloromethane T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
1: N-decylacetamide With triphenyl phosphite; chlorine; triethylamine in dichloromethane T=-30°C; 2: methanol in dichloromethane T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
Ferdani, Riccardo; Pajewski, Robert; Djedovic, Natasha; Pajewska, Jolanta; Schlesinger, Paul H.; Gokel, George W.
New Journal of Chemistry, 2005 , vol. 29, # 5 p. 673 - 680
potassium methanolate in methanol
T=40 - 45°C; electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 2.13 F mol-1; cell voltage 60-100 V; Yield given;
参考文献
Weiper-Idelmann, Andreas; Aus Dem Kahmen, Martin; Schaefer, Hans J.; Gockeln, Marianne
Acta Chemica Scandinavica, 1998 , vol. 52, # 6 p. 672 - 682
1: 72 percent / acetic acid
2: 1M potassium methoxide / methanol / 40 - 45 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 2.13 F mol-1; cell voltage 60-100 V
View Scheme
参考文献
Weiper-Idelmann, Andreas; Aus Dem Kahmen, Martin; Schaefer, Hans J.; Gockeln, Marianne
Acta Chemica Scandinavica, 1998 , vol. 52, # 6 p. 672 - 682
