3-丁基-4(3h)-喹唑啉酮合成路线 (共 15 条)
反应条件
2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; regioselective reaction;
参考文献
Punthasee, Puminun; Vanitcha, Avassaya; Wacharasindhu, Sumrit
Tetrahedron Letters, 2010 , vol. 51, # 13 p. 1713 - 1716
反应条件
Bi(OTf)3; 1-n-butylpyridinium tetrachloroferrate T=60°C; 0.0833333 h;
参考文献
Khosropour, Ahmad R.; Mohammadpoor-Baltork, Iraj; Ghorbankhani, Hamid
Tetrahedron Letters, 2006 , vol. 47, # 21 p. 3561 - 3564
反应条件
iodine T=80°C; 0.5 h; Ionic liquid;
参考文献
Wang, Shu-Liang; Yang, Ke; Yao, Chang-Sheng; Wang, Xiang-Shan.
Synthetic Communications, 2012 , vol. 42, # 3 p. 341 - 349
参考文献
Farzipour, Soghra; Saeedi, Mina; Mahdavi, Mohammad; Yavari, Hossein; Mirzahekmati, Mohammadreza; Ghaemi, Nasser; Foroumadi, Alireza; Shafiee, Abbas
Synthetic Communications, 2014 , vol. 44, # 4 p. 481 - 487
反应条件
boron trifluoride; silica gel T=20°C; 0.25 h; neat (no solvent);
参考文献
Wu, Liqiang; Ma, Weiwei; Yang, Limin; Yan, Fulin
Asian Journal of Chemistry, 2010 , vol. 22, # 8 p. 6053 - 6058
反应条件
1-methyl-3-(2-hydroxyl-3-acetoxylpropyl)imidazolium tetrafluoroborate; tetrabutylammomium bromide; potassium hydroxide in water; toluene 1 h; Reflux; Reagent/catalyst;
参考文献
Liu; Ji; Sun; Wen; Xu
Asian Journal of Chemistry, 2013 , vol. 25, # 17 p. 9853 - 9856
参考文献
Bogert; May
Journal of the American Chemical Society, 1909 , vol. 31, p. 512
反应条件
1: 95 percent / dimethylformamide / Heating 2: 61 percent / p-toluene-sulfonic acid / dioxane / 2 h / Heating; other benzoate and amines View Scheme
参考文献
Liu; Ji; Sun; Wen; Xu
Asian Journal of Chemistry, 2013 , vol. 25, # 17 p. 9853 - 9856
反应条件
toluene-4-sulfonic acid in 1,4-dioxane 2 h; Heating;
参考文献
Gupton, John T.; Miller, John F.; Bryant, Robert D.; Maloney, Patrick R.; Foster, Bruce S.
Tetrahedron, 1987 , vol. 43, # 8 p. 1747 - 1752
反应条件
1: platinum; ethanol / Hydrogenation 2: 170 °C View Scheme
参考文献
Leonard; Ruyle
Journal of Organic Chemistry, 1948 , vol. 13, p. 903,908