in further solvent(s) byproducts: ((C6H2(CH3)3)3PBr)[AlBr4]; in bromobenzene; stirred rapidly for 2 d at 25°C; vapor diffusion of cyclohexane into soln.;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 36 p. 8396 - 8399
in o-di-fluorobenzene byproducts: ((C6H2(CH3)3)3PI)[AlI4]; stirred rapidly for 4 d, slowly cooled to -38°C;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 36 p. 8396 - 8399
→
反应条件
in further solvent(s) Kinetics; in bromobenzene; at room temp. for 5 h; not isolated, detected by NMR, IR;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 36 p. 8396 - 8399
→
反应条件
in solid matrix Irradiation (UV/VIS); evapn. of U/(13)C/C (1:2:2) pellet by YAG laser with condensation at 8 Kfor 60 min, annealing to 20 and then to 30 K, irradiation at >290 nm fo r 20 min, annealing to 30 K and then to 35 K; IR monitoring;
参考文献
Journal of the American Chemical Society, , vol. 132, # 24 p. 8484 - 8488
