反-3,7-二甲基-2,6-辛二烯乙酸酯合成路线 (共 9 条)
反应条件
Rasta resin-(1,5,7-triazabicyclo[4.4.0]dec-5-ene)[RR-TBD] in tetrahydrofuran T=20 - 60°C;
参考文献
Yang, Yun-Chin; Leung, Dennis Y.C.; Toy, Patrick H.
Synlett, 2013 , vol. 24, # 14 art. no. ST-2013-W0412-L, p. 1870 - 1874
反应条件
iron(III) tosylate hexahydrate in acetonitrile T=0°C; 22.5 h;
参考文献
Baldwin, Neil J.; Nord, Anna N.; O'Donnell, Brendan D.; Mohan, Ram S.
Tetrahedron Letters, 2012 , vol. 53, # 51 p. 6946 - 6949
反应条件
[Zn(BH4)2(nmi)] in tetrahydrofuran T=20°C; 1 h; regioselective reaction;
参考文献
Setamdideh, Davood; Khezri, Behrooz
Asian Journal of Chemistry, 2010 , vol. 22, # 7 p. 5766 - 5772
反应条件
pseudomonas fluorescens lipase in acetonitrile T=30 - 32°C; 72 h; Enzymatic reaction;
参考文献
Gupta, Pankaj; Taneja, Subhash C.; Shah, Bhahwal A.; Sethi, Vijay K.; Qazi, Ghulam N.
Chemistry Letters, 2007 , vol. 36, # 9 p. 1110 - 1111
反应条件
triphenylphosphine in acetonitrile T=20°C; 24 h; Inert atmosphereDarkness; Reagent/catalyst;
参考文献
Nolla-Saltiel, Roberto; Carrillo-Arcos, Ulises Alonso; Porcel, Susana
Synthesis (Germany), 2014 , vol. 46, # 2 p. 165 - 169
反应条件
C12F18O13Zn4 24 h; RefluxInert atmosphere;
参考文献
Iwasaki, Takanori; Maegawa, Yusuke; Hayashi, Yukiko; Ohshima, Takashi; Mashima, Kazushi
Synlett, 2009 , # 10 p. 1659 - 1663
反应条件
decacarbonyldimanganese (2) in dichloromethane Radical coupling; UV-irradiation; Title compound not separated from byproducts;
参考文献
Gilbert, Bruce C.; Lindsay, Chris I.; McGrail, P. Terry; Parsons, Andrew F.; Whittaker, David T.E.
Synthetic Communications, 1999 , vol. 29, # 15 p. 2711 - 2718
反应条件
in acetonitrile T=20°C; 1.5 h; Inert atmosphereDarkness;
参考文献
Nolla-Saltiel, Roberto; Carrillo-Arcos, Ulises Alonso; Porcel, Susana
Synthesis (Germany), 2014 , vol. 46, # 2 p. 165 - 169
反应条件
potassium carbonate in methanol Inert atmosphere;
参考文献
Fischer, Daniel F.; Barakat, Assem; Xin, Zhuo-Qun; Weiss, Matthias E.; Peters, Rene
Chemistry - A European Journal, 2009 , vol. 15, # 35 p. 8722 - 8741