P,P-二(3,5-二甲基苯基)-N,N-二乙基亚膦酰胺合成路线 (共 18 条)
参考文献
Maier,L.
Helvetica Chimica Acta, 1969 , vol. 52, p. 858 - 871
反应条件
in acetonitrile T=45°C; 2 h;
参考文献
Ivanov, B. E.; Krokhina, S. S.; Chichkanova, T. V.; Ageeva, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 12 p. 2535 - 2539
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 12 p. 2765 - 2769
反应条件
in Petroleum ether T=90 - 100°C; 2.5 h;
参考文献
Ivanov, B. E.; Krokhina, S. S.; Chichkanova, T. V.; Kosacheva, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 1 p. 162 - 167
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 1 p. 173 - 178
反应条件
hydrogenchloride 0.75 h;
参考文献
RajanBabu; Ayers, Timothy A.; Halliday, Gary A.; You, Kimberly K.; Calabrese, Joseph C.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 6012 - 6025
反应条件
T=100°C; 1 h; Yield given;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 8, p. 235 - 242
反应条件
in dichloromethane
T=40°C; 1 h;
参考文献
Shintou, Taichi; Kikuchi, Wataru; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 8 p. 1645 - 1667
反应条件
sulfur dioxide in diethyl ether
参考文献
Denney,D.B. et al.
Journal of the American Chemical Society, 1969 , vol. 91, p. 5243 - 5246
反应条件
1: 80 percent / benzene / ice cooling
2: air
View Scheme
参考文献
Horner, Leopold; Jordan, Manfred
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 235 - 242