hydrogenchloride in pentane pumping HCl through soln. of trialkoxide at ambient temp. for 12 s yielded monochloride; pumping HCl for 30 s yielded dichloride; monitoring by 51V-NMR;
参考文献
Crans, Debbie C.; Chen, Haojiang; Felty, Robert A.
Journal of the American Chemical Society, 1992 , vol. 114, # 12 p. 4543 - 4550