(R)-1-苯基-1,2-乙二醇合成路线 （共 159 条）
反应条件
hydrogen; chiral iridium(III) complex in methanol T=60°C; P=7600.51 Torr; 15 h;
参考文献
Ohkuma, Takeshi; Utsumi, Noriyuki; Watanabe, Masahito; Tsutsumi, Kunihiko; Arai, Noriyoshi; Murata, Kunihiko
Organic Letters, 2007 , vol. 9, # 13 p. 2564 - 2567
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.5 h;
参考文献
Atobe, Masakazu; Yamazaki, Naoki; Kibayashi, Chihiro
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5595 - 5607
反应条件
D-glucose; D-glucose dehydrogenase; NADPH; carbonyl reductase from Pichia pastoris GS115; sodium hydroxide in aq. phosphate buffer; dimethyl sulfoxide T=20°C; pH=6.5; 12 h; Enzymatic reaction;
参考文献
Li, Zhe; Liu, Weidong; Chen, Xi; Jia, Shiru; Wu, Qiaqiang; Zhu, Dunming; Ma, Yanhe
Tetrahedron, 2013 , vol. 69, # 17 p. 3561 - 3564
反应条件
diisobutylaluminium hydride; (S)-1-methyl-2-lt;(piperidin-1-yl)-methylgt;pyrrolidine; tin(ll) chloride in dichloromethane T=-100°C; 0.333333 h; asymmetric reduction of prochiral hydroxy ketones; Product distribution;
参考文献
Chemistry Letters, , p. 1359 - 1362
反应条件
lithium aluminium tetrahydride in diethyl ether 1.) reflux, 5 h, 2.) RT, 12 h;
参考文献
Iuliano; Pini; Salvadori
Tetrahedron Asymmetry, 1995 , vol. 6, # 3 p. 739 - 744
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran T=0 - 20°C; 48 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
1: With water; 4-nitro-benzoic acid; Jacobsen's (S,S)-(salen)Co(III) catalyst T=20°C; Acidic aqueous solution; 2: With ammonia T=20°C; 1 h;
参考文献
WO2004/20429 A1, ;
Page 38-39 ;
反应条件
1,4-bis(9-O-dihydroquinidine)phthalazine in water; tert-butyl alcohol T=20°C; Sharpless asymmetric dihydroxylation; 2 h;
参考文献
Branco, Luis C.; Ferreira, Frederico Castelo; Santos, Jose L.; Crespo, Joao G.; Afonso, Carlos A. M.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 2086 - 2098
反应条件
potassium dioxotetrahydroxoosmate(VI); potassium carbonate; potassium hexacyanoferrate(III); methanesulfonamide; DHQD-PHAL-OPEG-OMe in water; tert-butyl alcohol T=0°C; 24 h; Title compound not separated from byproducts;
参考文献
Kuang, Yong-Qing; Zhang, Sheng-Yong; Wei, Ling-Ling
Tetrahedron Letters, 2001 , vol. 42, # 34 p. 5925 - 5927
反应条件
trislt;trinitratocerium(IV)gt; paraperiodate; water in acetonitrile 0.0833333 h; Ambient temperature;
参考文献
Iranpoor; Zardaloo
Synthetic Communications, 1994 , vol. 24, # 14 p. 1959 - 1969
