1,3,2-二氧杂磷杂环己烷-2-氧化物合成路线 （共 14 条）
反应条件
potassium carbonate; 18-crown-6 ether in 1,4-dioxane 12 h; Heating;
参考文献
Yuan; Li; Cheng
Synthesis, 1988 , vol. 1, # 3 p. 186 - 189
反应条件
in tetrahydrofuran
T=70°C; 2 h; Inert atmosphere;
参考文献
Gosset, Gaelle; Clement, Jean-Louis; Culcasi, Marcel; Rockenbauer, Antal; Pietri, Sylvia
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 7 p. 2218 - 2230
反应条件
in dichloromethane
T=0°C; 8 h;
参考文献
Academia Sinica; Wong, Chi-Huey; Fang, Jim-Min; Liu, Kung-Cheng; Jan, Jia-Tsrong; Cheng, Yih-Shyun E.; Cheng, Ting-Jen R.
Patent: US2013/274229 A1, 2013 ;
Location in patent: Paragraph 0314 ;
反应条件
phosphonic acid; dicyclohexyl-carbodiimide in tetrahydrofuran
T=20°C; Esterification;
参考文献
Munoz, Aurelio; Hubert, Cathy; Luche, Jean-Louis
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 6015 - 6017
反应条件
T=130 - 140°C; P=150 Torr; 4 h;
参考文献
Maffei, Michel; Buono, Gerard
Tetrahedron, 2003 , vol. 59, # 44 p. 8821 - 8825
反应条件
orthophosphorus acid; acetic anhydride in 1,4-dioxane
2 h; Heating;
参考文献
Klosinski
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2025 - 2028
反应条件
propylamine in chloroform-d1
T=25°C;
参考文献
Wada, Takeshi; Honda, Fumio; Sato, Yuichi; Sekine, Mitsuo
Tetrahedron Letters, 1999 , vol. 40, # 5 p. 915 - 918
反应条件
in benzene
Irradiation;
参考文献
Omelanzcuk, Jan; Sopchik, Alan E.; Lee, Sueg-Geun; Akutagawa, Kunihiko; Cairns, Matthew S.; Bentrude, Wesley G.
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6908 - 6909
反应条件
water; triethylamine; benzene
Reagens 4:Tetrahydrofuran;
参考文献
Zwierzak,A.
Canadian Journal of Chemistry, 1967 , vol. 45, p. 2501 - 2512
反应条件
dimethyl amine in diethyl ether
参考文献
Munoz,A. et al.
Bulletin de la Societe Chimique de France, 1971 , p. 1424 - 1436
