3-苯基-4-(3H)喹啉酮合成路线 (共 45 条)
反应条件
oxygen in dimethyl sulfoxide T=120°C; 48 h;
参考文献
Kim, Na Yeun; Cheon, Cheol-Hong
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2340 - 2344
反应条件
ytterbium(III) triflate T=60°C; 0.0333333 h;
参考文献
Wang, Min; Song, Zhiguo; Zhang, Tingting
Synthetic Communications, 2011 , vol. 41, # 3 p. 385 - 391
反应条件
ytterbium(III) triflate T=60°C; 0.0333333 h;
参考文献
Wang, Limin; Xia, Jianjun; Qin, Fang; Qian, Changtao; Sun, Jie
Synthesis, 2003 , # 8 p. 1241 - 1247
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate T=20°C; 0.116667 h; Ionic liquidSonication;
参考文献
Pawar, Omprakash B.; Chavan, Fulchand R.; Sakate, Sachin S.; Shinde, Narayan D.
Chinese Journal of Chemistry, 2010 , vol. 28, # 1 p. 69 - 71
反应条件
1: 2-bromophenyl isocyanide With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.25 h; Inert atmosphere; 2: phenyl isocyanate in tetrahydrofuran; hexane T=-78°C; 3 h; Inert atmosphere; 3: With water; ammonium chloride in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Lygin, Alexander V.; De Meijere, Armin
Organic Letters, 2009 , vol. 11, # 2 p. 389 - 392
反应条件
copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine in N,N-dimethyl-formamide T=80°C; 24 h; Inert atmosphere;
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=20 - 75°C;
参考文献
Xiao, Zili; Yang, Michael G.; Li, Peng; Carter, Percy H.
Organic Letters, 2009 , vol. 11, # 6 p. 1421 - 1424
反应条件
iodine T=80°C; 0.75 h; Ionic liquid;
参考文献
Wang, Shu-Liang; Yang, Ke; Yao, Chang-Sheng; Wang, Xiang-Shan.
Synthetic Communications, 2012 , vol. 42, # 3 p. 341 - 349
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; di-(1-adamantyl)-n-butylphosphine in 1,4-dioxane T=100°C; P=7500.75 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
He, Lin; Li, Haoquan; Neumann, Helfried; Beller, Matthias; Wu, Xiao-Feng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 5 p. 1420 - 1424
Angew. Chem., 2014 , vol. 126, # 5 p. 1444 - 1448,5
反应条件
titanium tetrachloride; zinc in tetrahydrofuran Heating;
参考文献
Shi, Daqing; Shi, Chunling; Wang, Juxian; Rong, Liangce; Zhuang, Qiya; Wang, Xiangshan
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 2 p. 173 - 183