2,6-二羟基-4-甲基苯乙酮合成路线 （共 21 条）
反应条件
aluminium trichloride in chlorobenzene T=90°C; Fries rearrangement; deacetylation; 1 h;
参考文献
Tsujihara, Kenji; Hongu, Mitsuya; Saito, Kunio; Kawanishi, Hiroyuki; Kuriyama, Kayoko; Matsumoto, Mamoru; Akira, Oku; Ueta, Kiichiro; Tsuda, Minoru; Saito, Akira
Journal of Medicinal Chemistry, 1999 , vol. 42, # 26 p. 5311 - 5324
反应条件
AlCl3, aluminium chloride in chlorobenzene T=40 - 70°C; 1.5 h; Inert atmosphere;
参考文献
Qin, Tian; Johnson, Richard P.; Porco, John A.
Journal of the American Chemical Society, 2011 , vol. 133, # 6 p. 1714 - 1717
反应条件
potassium hydroxide in ethanol T=40°C; 0.5 h;
参考文献
Archiv der Pharmazie, , vol. 318, # 4 p. 328 - 340
参考文献
Proceedings - Indian Academy of Sciences, Section A, , vol. <A> 29, p. 269,270
Proceedings - Indian Academy of Sciences, Section A, , vol. 25, p. 353,356
Proceedings - Indian Academy of Sciences, Section A, , vol. 29, p. 269,272
反应条件
aluminium trichloride in chlorobenzene T=90°C; Fries rearrangement;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 20 p. 5121 - 5125
反应条件
1: 2,6-bis(trimethylsilyloxy)-4-methylacetophenone With sodium hydride in tetrahydrofuran; mineral oil T=20 - 75°C; 2: ethyl acetate in tetrahydrofuran; mineral oil T=20 - 75°C; Aldol condensation;
参考文献
Koenigs; Rinker; Maus; Nieger; Rheinheimer; Waldvogel
Journal of Natural Products, 2010 , vol. 73, # 12 p. 2064 - 2066
反应条件
1: pyridine 2: AlCl3 / chlorobenzene / 90 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 20 p. 5121 - 5125
反应条件
trichlorophosphate T=100 - 110°C; Giessen in Wasser,Loesen des gefaellten Oels in kochender verd.Natronlauge, Faellen der Loesung mit Salzsaeure, Umkristallisieren des Niederschlags aus Benzol;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 26, p. 62
反应条件
boron trifluoride diethyl etherate T=0 - 20°C;
参考文献
Journal of Molecular Structure, , vol. 936, # 1-3 p. 277 - 282
参考文献
Journal of the South African Chemical Institute, , vol. 26, p. 41,45
