3,4-二苯基-1H-吡咯合成路线 （共 16 条）
反应条件
trichlorophosphate T=70°C; 1 h;
参考文献
Dannhardt; Steindl
Archiv der Pharmazie, 1986 , vol. 319, # 8 p. 749 - 755
反应条件
nickel dichloride in N,N-dimethyl acetamide
T=110°C; 4 h; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Chen, Feng; Shen, Tao; Cui, Yuxin; Jiao, Ning
Organic Letters, 2012 , vol. 14, # 18 p. 4926 - 4929,4
反应条件
copper(l) iodide; caesium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in 1,4-dioxane
20 h; Heating;
参考文献
Yuan, Xiyuan; Xu, Xiaobing; Zhou, Xiaobo; Yuan, Jiwei; Mai, Lugen; Li, Yanzhong
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1510 - 1513
反应条件
titanium(III) chloride in 1,4-dioxane; water
T=35°C; 24 h; pH 6.5;
参考文献
Ono, Noboru; Miyagawa, Hirokazu; Ueta, Takahiro; Ogawa, Takuji; Tani, Hiroyuki
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1595 - 1601
反应条件
nickel dichloride in N,N-dimethyl acetamide
T=110°C; 4 h; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Chen, Feng; Shen, Tao; Cui, Yuxin; Jiao, Ning
Organic Letters, 2012 , vol. 14, # 18 p. 4926 - 4929,4
反应条件
potassium tert-butylate in ethylene glycol dimethyl ether
T=0 - 20°C; 1 h;
参考文献
Leusen, Daan van; Echten, Erik van; Leusen, Albert M. van
Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2245 - 2249
反应条件
sodium hydroxide in ethylene glycol
T=170°C; 2 h;
参考文献
Ono, Noboru; Miyagawa, Hirokazu; Ueta, Takahiro; Ogawa, Takuji; Tani, Hiroyuki
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1595 - 1601
反应条件
1: With ammonia in tetrahydrofuran
T=20°C; 0.5 h;
2: With silver(I) acetate; sodium acetate in tetrahydrofuran
T=60°C; 80 h;
参考文献
Li, Qingjiang; Fan, Aili; Lu, Zhiyao; Cui, Yuxin; Lin, Wenhan; Jia, Yanxing
Organic Letters, 2010 , vol. 12, # 18 p. 4066 - 4069
反应条件
diisobutylaluminium hydride in toluene; benzene
T=20°C; 6 h;
参考文献
Ramirez-Rodriguez, Armando; Mendez, Jose M.; Jimenez, Cristina C.; Leon, Fernando; Vazquez, Alfredo
Synthesis, 2012 , vol. 44, # 21 art. no. SS2012M0512OP, p. 3321 - 3326,6
反应条件
copper(l) iodide; caesium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in 1,4-dioxane
4 h; Heating;
参考文献
Li, Ende; Xu, Xiaobing; Li, Hongfeng; Zhang, Huimin; Xu, Xiaolei; Yuan, Xiyuan; Li, Yanzhong
Tetrahedron, 2009 , vol. 65, # 44 p. 8961 - 8968
