1-(4-氯苯基)-1H-吡咯-2,5-二酮合成路线 (共 17 条)
反应条件
1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride in benzene 5 h; Heating / reflux;
参考文献
Boehringer, Markus; Zbinden, Katrin Groebke; Haap, Wolfgang; Hilpert, Hans; Himber, Jacques; Humm, Roland; Iding, Hans; Knopp, Dietmar; Panday, Narendra; Ricklin, Fabienne; Stahl, Christoph Martin
Patent: US2006/106016 A1, 2006 ;
Location in patent: Page/Page column 42 ;
反应条件
1-n-butyl-3-methylimidazolium hexafluorophosphate T=140°C; 0.333333 h;
参考文献
Le, Zhang-Gao; Chen, Zhen-Chu; Hu, Yi; Zheng, Qin-Guo
Synthesis, 2004 , # 7 p. 995 - 998
反应条件
triethylamine in water; benzene
反应条件
triethylamine in acetone 2 h;
参考文献
Gaina, Constantin; Gaina, Viorica
Revue Roumaine de Chimie, 2005 , vol. 50, # 7-8 p. 655 - 661
反应条件
1: chloroform / 1 h / 20 °C 2: sodium acetate; acetic anhydride / 2 h / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 9 p. 2823 - 2834
反应条件
acetic acid T=100°C; 1.5 h;
参考文献
Kumar, Padam Praveen; Mohiuddin; Rama Devi; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 5 p. 686 - 690
反应条件
acetic acid T=100°C; 1.33333 h;
参考文献
Kumar, Padam Praveen; Mohiuddin; Rama Devi; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 5 p. 686 - 690
反应条件
thionyl chloride; triethylamine in tetrahydrofuran T=20°C; 6.5 h; Reflux;
参考文献
Faturaci, Yeliz; Coskun, Necdet
Turkish Journal of Chemistry, 2012 , vol. 36, # 5 p. 749 - 758
反应条件
sodium acetate; acetic anhydride T=100°C;
参考文献
Chemistry - A European Journal, , vol. 16, # 42 p. 12534 - 12537
反应条件
sulfuric acid T=60°C;
参考文献
Organic Preparations and Procedures International, , vol. 45, # 4 p. 314 - 320