6-甲基-1H-吲哚-3-羧酸甲酯合成路线 （共 4 条）
反应条件
aluminium trichloride in dichloromethane T=25°C;
参考文献
Hirano, Satoshi; Akai, Ritsuko; Shinoda, Yoshihiko; Nakatsuka, Shin-ichi
Heterocycles, 1995 , vol. 41, # 2 p. 255 - 258
反应条件
1: 96 percent / K2CO3 / dimethylformamide 2: 31 percent / Br2 / 2 h / 0 °C 3: 91 percent / AlCl3 / CH2Cl2 / 0.5 h / -20 °C 4: 76 percent / Raney Ni / methanol / 0.17 h / 25 °C 5: 87 percent / AlCl3 / CH2Cl2 / 25 °C View Scheme
参考文献
Hirano, Satoshi; Akai, Ritsuko; Shinoda, Yoshihiko; Nakatsuka, Shin-ichi
Heterocycles, 1995 , vol. 41, # 2 p. 255 - 258
反应条件
1: 31 percent / Br2 / 2 h / 0 °C 2: 91 percent / AlCl3 / CH2Cl2 / 0.5 h / -20 °C 3: 76 percent / Raney Ni / methanol / 0.17 h / 25 °C 4: 87 percent / AlCl3 / CH2Cl2 / 25 °C View Scheme
参考文献
Hirano, Satoshi; Akai, Ritsuko; Shinoda, Yoshihiko; Nakatsuka, Shin-ichi
Heterocycles, 1995 , vol. 41, # 2 p. 255 - 258
反应条件
1: 91 percent / AlCl3 / CH2Cl2 / 0.5 h / -20 °C 2: 76 percent / Raney Ni / methanol / 0.17 h / 25 °C 3: 87 percent / AlCl3 / CH2Cl2 / 25 °C View Scheme
参考文献
Hirano, Satoshi; Akai, Ritsuko; Shinoda, Yoshihiko; Nakatsuka, Shin-ichi
Heterocycles, 1995 , vol. 41, # 2 p. 255 - 258
