反应条件
in diethyl ether
N2-atmosphere; addn. of 2 equiv. dithiol to B-compd. at 0°C, standing for 5 min; dropwise addn. of excess 1 M HCl in Et2O, stirring for 24 h, solvent removal (vac.), extn. into PhMe, filtration (Celite), crystn. (5°C, 12 h); elem. anal.;
参考文献
Lawlor, Fiona J.; Norman, Nicholas C.; Pickett, Nigel L.; Robins, Edward G.; Nguyen, Paul; Lesley, Gerry; Marder, Todd B.; Ashmore, Jennifer A.; Green, Jennifer C.
Inorganic Chemistry, 1998 , vol. 37, # 20 p. 5282 - 5288
