2,4-二氯-1,3,5-三硝基苯合成路线 （共 19 条）
反应条件
sulfuric acid; nitric acid
参考文献
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5> 18 I, p. 101
参考文献
Journal of the Indian Chemical Society, , vol. 9, p. 59,63
反应条件
sodium in neat (no solvent)
参考文献
Dutta, Pradeep K.; Bagchi, Debasis; Pakrashi, Satyesh C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 11 p. 1037 - 1038
反应条件
ammonia in toluene
Heating;
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1909 , vol. <5> 18 I, p. 101
反应条件
1: 92 percent / sodium azide / dimethylformamide; H2O / 3.5 h / 20 - 22 °C
2: 77 percent / acetic acid / 2 h / Heating
View Scheme
参考文献
Mehilal; Sikder; Salunke
New Journal of Chemistry, 2001 , vol. 25, # 12 p. 1549 - 1552
反应条件
1: sodium / neat (no solvent)
2: 35 percent / hydrogen / PtO2 / ethanol / 0.17 h / 2585.7 - 2844.3 Torr / Ambient temperature
3: 40 percent / HCl, SnCl2 / H2O / 30 h / 120 - 122 °C / sealed tube
4: 85 percent / dry HCl, anhydrous ZnCl2 / diethyl ether / 48 h
5: 1.) triethylamine, 2.) KOH / 1.) 5 h, 160 - 180 deg C, 2.) aq. ethanol, 30 min, reflux
View Scheme
参考文献
Dutta, Pradeep K.; Bagchi, Debasis; Pakrashi, Satyesh C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 11 p. 1037 - 1038
反应条件
1: 90 percent / NH3 / toluene / Heating
2: H2 / 10percent Pd/C / methanol / 3000.2 Torr / Ambient temperature
View Scheme
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
参考文献
Heidberg,J.; Weil,J.A.
Journal of the American Chemical Society, 1964 , vol. 86, p. 5173 - 5174
