2,4,6-三硝基苯-1,3-二胺合成路线 （共 46 条）
参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1908 , vol. <5> 17 I, p. 473
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Noelting; Collin
Chemische Berichte, 1884 , vol. 17, p. 265
参考文献
Barr
Chemische Berichte, 1888 , vol. 21, p. 1543
Full Text Show Details
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1908 , vol. <5> 17 I, p. 473
Full Text Show Details
Noelting; Collin
Chemische Berichte, 1884 , vol. 17, p. 265
反应条件
ammonia in water
T=123°C; 1 h;
参考文献
The Regents of the University of California.
Patent: US2005/38297 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: With sodium methylate in methanol; dimethyl sulfoxide; toluene
T=25 - 90°C; 2.33333 h;
2: With acetic acid in dimethyl sulfoxide; toluene
Product distribution / selectivity;
参考文献
The Regents of the University of California.
Patent: US2005/38297 A1, 2005 ;
Location in patent: Page/Page column 4 ;
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
反应条件
ammonia in toluene
Heating;
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
反应条件
methanol; hydroxylamine; sodium methylate
参考文献
Meisenheimer; Patzig
Chemische Berichte, 1906 , vol. 39, p. 2540
参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1908 , vol. <5> 17 I, p. 473
反应条件
1: 96 percent / 100percent HNO3, 96percent H2SO4 / 1 h / 90 °C
2: 95 percent / NH3 / methanol
View Scheme
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
反应条件
1: 68 percent / KNO3, 30percent oleum / 12 h / 120 °C
2: 90 percent / NH3 / toluene / Heating
View Scheme
参考文献
Praefcke, Klaus; Kohne, Bernd; Korinth, Frank; Psaras, Panicos; Nasielski, Jaques; et al.
Liebigs Annalen der Chemie, 1989 , p. 617 - 622
