chlorine in tetrachloromethane byproducts: CoCl2; under N2 a soln. of Co-complex in CCl4 was treated with a soln. of Cl2 in CCl4 at room temp. for 15 min; monitored by IR, pumped off, extd. with n-pentane, evapd.;
参考文献
Journal of Organometallic Chemistry, , vol. 205, # 1 p. 31 - 45
in benzene compds. stirred together in refluxing benzene for 3 h; cooled to room temp., filtered, washed with benzene to give PhTe(NPPh3)Cl2, combined filtrate and washings concd. to give Ph3GeCl;
参考文献
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, , vol. 12, p. 47 - 54
