反应条件
in melt according to F. Rijkens, G.J.M. van der Kerk, Rec. Trav. Chim. 83 (1964)723; under dry O2-free Ar using Schlenk techniques; mixt. of Ph4Ge (5.35mmol), AlCl3 (0.49 mmol) and GeCl4 (1.60 mmol) heated (120°C, 4 h); cooled to room temp.; recrystd. from hexane;
参考文献
Zaitsev, Kirill V.; Kapranov, Andrey A.; Oprunenko, Yuri F.; Churakov, Andrei V.; Howard, Judith A.K.; Tarasevich, Boris N.; Karlov, Sergey S.; Zaitseva, Galina S.
Journal of Organometallic Chemistry, 2012 , vol. 700, p. 207 - 213
