9,10-二氢-9,10-乙烯桥蒽-11,12-二甲酸酐合成路线 （共 5 条）
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=0 - 20°C;
参考文献
Bouffard, Jean; Eaton, Robert F.; Mueller, Peter; Swager, Timothy M.
Journal of Organic Chemistry, 2007 , vol. 72, # 26 p. 10166 - 10180
反应条件
1: NaOH; H2O / methanol / 1 h / Heating 2: Ac2O; NaOAc / 0.5 h / 80 °C View Scheme
参考文献
Okamoto, Iwao; Ohwada, Tomohiko; Shudo, Koichi
Journal of Organic Chemistry, 1996 , vol. 61, # 9 p. 3155 - 3166
反应条件
1: 64 percent / 22 h / 110 °C 2: 97 percent / aq. NaOH / methanol / 6 h / 60 °C 3: 85 percent / acetic anhydride / 5 h / 70 °C / further reagents: thionyl chloride, pyridine View Scheme
参考文献
Smet, Mario; Corens, David; Van Meervelt, Luc; Dehaen, Wim
Molecules, 2000 , vol. 5, # 2 p. 179 - 188
参考文献
Chatervedi; Verma
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 9 - 13
参考文献
Diels; Alder
Justus Liebigs Annalen der Chemie, 1931 , vol. 486, p. 217,225
Justus Liebigs Annalen der Chemie, 1932 , vol. 498, p. 7,9,11
