反应条件
1.1: acetic acid; tin / 3 h / 100 - 120 °C 2.1: potassium carbonate / acetone; water / 4 h / 10 - 50 °C / |Cooling 3.1: magnesium; iodine / tetrahydrofuran / 5 h / |Reflux 3.2: 1.75 h / 10 - 90 °C 3.3: 1 h / 20 °C 4.1: sodium hydroxide / water / 4 h 5.1: hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr View Scheme
参考文献
Prabhakar; Reddy, C. Bakki; Reddy, Ch. Maheedhara; Nageshwar; Devi, A. Sivalakshmi; Babu, J. Moses; Vyas; Sarma; Reddy
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 121 - 125
