1-苯基-2-(4-吡啶)乙酮合成路线 （共 44 条）
反应条件
2,2'-azo-bisisobutyronitrile in tetrachloromethane
16 h; Heating; Yield given;
参考文献
Lee, Cheuk Man; Sammes, Michael P.; Katritzky, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2458 - 2462
反应条件
1: ethanolic KOH-solution
2: sulfuric acid; water
View Scheme
参考文献
Lukes; Ernest
Collection of Czechoslovak Chemical Communications, 1949 , vol. 14, p. 665,672
反应条件
1: methanol; N,N-dimethyl-4-nitroso-aniline / und anschliessend mit wss.Natronlauge unter Stickstoff
2: hydrobromic acid; water / 180 °C / unter Druck
View Scheme
参考文献
Kroehnke et al.
Justus Liebigs Annalen der Chemie, 1956 , vol. 600, p. 176,188
反应条件
1: pyridine; potassium permanganate; water
2: hydrobromic acid; water / 180 °C / unter Druck
View Scheme
参考文献
Kroehnke et al.
Justus Liebigs Annalen der Chemie, 1956 , vol. 600, p. 176,188
反应条件
1: chloroform; water / und anschliessend mit wss.Natronlauge
2: hydrobromic acid; water / 180 °C / unter Druck
View Scheme
参考文献
Kroehnke et al.
Justus Liebigs Annalen der Chemie, 1956 , vol. 600, p. 176,188
反应条件
lithium diisopropyl amide; dibenzoyl peroxide
1) THF, -78 deg C, 20 min, 2a) THF, -78 deg C, 2h, 2b) RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jahangir; Wang; Smith; MacLean; Holland
Canadian Journal of Chemistry, 1990 , vol. 68, # 4 p. 587 - 591
反应条件
lithium diisopropyl amide
1) THF, -78 deg C, 20 min, 2a) THF, -78 deg C, 2h, 2b) RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jahangir; Wang; Smith; MacLean; Holland
Canadian Journal of Chemistry, 1990 , vol. 68, # 4 p. 587 - 591
反应条件
2,2'-azo-bisisobutyronitrile in tetrachloromethane
16 h; Heatingeffect of solvent and presence of various initiators or free-radical quencher; Product distributionMechanism;
参考文献
Lee, Cheuk Man; Sammes, Michael P.; Katritzky, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2458 - 2462
反应条件
anschliessend Behandeln mit Methylbenzoat;
参考文献
Osuch; Levine
Journal of Organic Chemistry, 1957 , vol. 22, p. 939,942
反应条件
anschliessend mit Methylbenzoat erwaermen;
参考文献
Osuch; Levine
Journal of Organic Chemistry, 1957 , vol. 22, p. 939,942
