tetrabutylammomium bromide in dichloromethane T=20°C; diaphragm cell, platinum cathode; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 6.2 p. 1332
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1451
→
反应条件
in N,N-dimethyl-formamide Electrolysis; a DMF soln. of ((Co(C2C3)(DO)(DOH)pn)(CH2C(CO2C2H5)2CH3)Br) and TBAF was subjected to electrolysis at -2.0 V vs. SCE in the dark for 8 h; detected by GLC;
参考文献
Murakami, Yukito; Hisaeda, Yoshio; Fan, Sheng-Di; Matsuda, Yoshihisa
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 7 p. 2219 - 2228
→
反应条件
in N,N-dimethyl-formamide Electrolysis; controlled-potential electrolysis at -1.5 V vs. SCE in DMF containing Bu4NF and AcOH at 20.5°C in the dark; not isolated; the reaction was monitored by electronic spectroscopy, ESR spin-trapping technique;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 1 p. 311 - 324
