甲磺酸-2-丙炔-1-醇合成路线 (共 22 条)
反应条件
1: undec-1-yne With ethyl magnesium chloride in tetrahydrofuran; diethyl ether
2 h; Heating;
2: methanesulfonic acid prop-2-ynyl ester With copper(l) iodide in tetrahydrofuran; diethyl ether
T=0 - 20°C; Further stages.;
参考文献
Kang, Baldip; Britton, Robert
Organic Letters, 2007 , vol. 9, # 24 p. 5083 - 5086
反应条件
in n-heptane; dichloromethane
T=0°C; 0.5 h;
参考文献
Kessabi, Jilali; Beaudegnies, Renaud; Jung, Pierre M. J.; Benjamin Martin, Florian Montel; Wendeborn, Sebastian
Synthesis, 2008 , # 4 p. 655 - 659