(2Z)-戊-2,4-二烯腈合成路线 (共 25 条)
反应条件
lithium hydroxide in acetonitrile T=40°C; Product distribution / selectivity;
参考文献
Degussa AG
Patent: US2003/212298 A1, 2003 ;
Location in patent: Page/Page column 3 ;
反应条件
diethyl ether Hydrieren des Reaktionsprodukts an Palladium in wss.Methanol und Erhitzen des Reaktionsprodukts mit wss.Salzsaeure;
参考文献
Celanese Corp. Am.
Patent: US2527509 , 1946 ;
反应条件
1: Edukt1 ist Gemisch der Stereoisomeren 2: palladium/charcoal; diethyl ether / Hydrogenation 3: Raney nickel; ethanolic ammonia / 100 °C / Hydrogenation.unter Druck View Scheme
参考文献
Stewart
Journal of the American Chemical Society, 1954 , vol. 76, p. 3228
反应条件
tetraethylammonium p-toluenesulfonate
参考文献
Baizer,M.M.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1670 - 1673
反应条件
2: palladium/charcoal; diethyl ether / Hydrogenation 3: Raney nickel; ethanolic NH3 / 100 °C / Hydrogenation.unter Druck View Scheme
参考文献
Journal of the American Chemical Society, , vol. 76, p. 3228
反应条件
1: Edukt1 ist Gemisch der Stereoisomeren 2: nickel Fuller's earth; ammonia; methanol / 100 °C / Hydrogenation.unter Druck View Scheme
参考文献
Lespagnol,A. et al.
Bulletin de la Societe Chimique de France, 1960 , p. 1162 - 1165
反应条件
1: Edukt1 ist Gemisch der Stereoisomeren 2: palladium/charcoal; diethyl ether / Hydrogenation 3: Raney nickel; ethanolic ammonia / 100 °C / Hydrogenation.unter Druck View Scheme
参考文献
Stewart
Journal of the American Chemical Society, 1954 , vol. 76, p. 3228
反应条件
recombinant nitrilase AtNIT1 from Arabidopsis thailana; Tris*HCl buffer in methanol; water T=20°C; pH=8.5; 24 h;
参考文献
Effenberger, Franz; Osswald, Steffen
Tetrahedron Asymmetry, 2001 , vol. 12, # 18 p. 2581 - 2587
反应条件
1: Edukt1 ist Gemisch der Stereoisomeren
2: palladium/charcoal; diethyl ether / Hydrogenation
3: Raney nickel; ethanolic ammonia / 100 °C / Hydrogenation.unter Druck
View Scheme
参考文献
Stewart
Journal of the American Chemical Society, 1954 , vol. 76, p. 3228
反应条件
platinum
Hydrogenation;
参考文献
Coffman
Journal of the American Chemical Society, 1935 , vol. 57, p. 1978